Ace Glass 7482-50 Shaker Type Hydrogenation/Gas Apparatus I 120V 60Hz

Shaker Type Hydrogenation/Gas Apparatus

These shakers provide a compact, easily operated system for treating chemicals with hydrogen in the presence of a catalyst at pressures up to four atmospheres (60 psig) and temperatures to 80°C. Apparatus I is used primarily for synthesizing or modifying organic compounds by catalytic hydrogenation, reduction or condensation, but are equally suitable for other laboratory procedures in which a liquid and gas must be mixed vigorously in a glass reactor at pressures up to four atmospheres. Apparatus I features heavy walled, pressure-tested glass reaction vessels and connectors modified with state-of-the-art closures - Ace-Threds - that eliminate the use of rubber stoppers. Tubing from the gas tank can be securely held by an O-Ring compression seal in a threaded adapter that in turn seals the reaction vessel. The vessels can be in different volumes up to 200 mL.

Three small-volume reactors are supplied with #7 Ace-Thred that accepts a Nylon bushing-spacer, 7482-31, with a #7 male thread at bottom to secure tubing from gas tank via an O-Ring compression seal. This bushing-spacer is used to take up the space between the vessel and the top of the shaker. Three larger-volume reactors supplied accept 7482-33 Adapter #25 to #7. Tubing is secured via 5029-202 Big Head #7 Bushing. These vessels are large enough to fill space to top of shaker.

The individual parts and glassware below, along with Hydrogenation/Gas Appartus I (7482-20), comprise the Complete Item listed above.

• Glass Vessel, #7 Ace-Thred, 8 mL - 8648-120
• Glass Vessel, #7 Ace-Thred, 14 mL - 8648-124
• Glass Vessel, #7 Ace-Thred, 25 mL - 8648-126
• Glass Vessel, #25 Ace-Thred, 75 mL - 8648-135
• Glass Vessel, #25 Ace-Thred, 175 mL - 8648-138
• Glass Vessel, #25 Ace-Thred, 325 mL - 8648-140
• Spacer-Bushing, Nylon, #7 Ace-Thred - 7482-31
• Bushing, Nylon, Big Head, #7 Ace-Thred - 5029-202
• Adapter, PTFE, #7-25 Ace-Thred - 7482-33
• Upper Rubber Pad - 7482-37
• Lower Rubber Pad - 7482-38
• Aluminum Mounting Frame - 7482-77

For more information, please see Brochure