Ace Glass 6474-75 Unjacketed Spherical Reactor System with Support Stand, 200 L

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Ace Glass 6474-75 Unjacketed Spherical Reactor System with Support Stand, 200 L
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  • $57,014.00 / Kit
    • $57,014.00 / Kit
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Overview


This system comprises a self-supporting mobile frame made from one-inch stainless steel pipe, measuring 90" in height, 42" in width, and 42" in depth. It arrives fully assembled.

The flask features a 300 mm (12") flat-ground flange opening and a bottom outlet with a flush seal drain valve equipped with one-inch beaded drain discharge. The valve O-Rings are CAPFE (silicone encapsulated with PTFE) and Kalrez® for superior chemical resistance. A 100 mm I.D. side port, angled at 45 degrees, is included.

The black epoxy-coated aluminum flask support plate is vertically adjustable, accommodating various outlet configurations, and upper support brackets are provided to stabilize the flask.

The head, boasting a traditional domed style, features seven openings: (5) 45/50 and (2) 29/42. The motor is securely positioned on a black epoxy-coated mounting plate over the central 45/50 opening, while other openings serve components like the condenser, thermoprobe, and cooling coil. The head is secured to the flask with a PTFE gasket and plastic coupling, with a maximum bolt tightening torque of 30 in-lbs. (in a cold state).

The stirring mechanism is powered by a heavy-duty 3/8 HP DC motor designed for non-hazardous area duty. The motor shaft measures 5/8" O.D., and the controller operates on 120 volts 50/60 Hz. An air motor option is available upon request. The system features a 28 mm (1-1/8") O.D. precision ground and polished glass stirring shaft, equipped with a multi-paddle PTFE agitator at the bottom and a turbine blade PTFE agitator higher on the shaft for grease-free operation with an 8067 PTFE bearing.

The cooling coil is constructed using 1/2" O.D. copper tubing encapsulated with PTFE.

To control heating mantles effectively, a digital temperature control system is included, preventing overheating and overshoot while offering an instant temperature readout.

Features:

  • 200 liter reactor with bottom outlet
  • Internal heat exchange coil
  • Rugged stainless steel pipe support frame on casters for mobility
  • Adjustable height flask support

The package includes:

  • FLASK, with Side Necks and 2 inch Beaded Pipe Bottom Opening  - 6474-29 
  • HEAD, Domed, with Seven Openings - 6472-23 
  • GASKET, PTFE - 6525-51 
  • COUPLING, with inserts and hardware - 6525-30 
  • WRENCH, Torque, 30 in-lbs - 6525-60 
  • SOCKET, 1/4 inch - 6525-61 
  • DRAIN VALVE, Flush Seal - 6472-245 
  • CLAMP, Drain Valve, 1 inch - 8856-07 
  • CLAMP, Drain Valve, 2 inch - 8856-11 
  • SWEEP ELBOW, 60°, 1 inch BP - 8830-207 
  • CAP, 4 inch - 15312-33 
  • O-Ring, CAPFE, for 4 inch Flange - 7855-880 
  • CLAMP, Quick Release - 6517-25 
  • MANTLE, Bottom, Aluminum, w/hole, 4-2000x-230v, wired with plugs - 12053-78 
  • SUPPORT ASSEMBLY, Complete - 6474-373 
  • TEMPERATURE CONTROL SYSTEM, Complete - 6472-83 
  • STIRRING MOTOR AND CONTROLLER, 1/2 HP - 13554-55 
  • AGITATOR, Lower, PTFE, Multipaddle, 178 mm - 8091-36 
  • AGITATOR, Upper, PTFE, with 4 Pitched Blades, 152 mm - 8093-35 
  • STIRRING SHAFT, Polished Glass, 28 mm - 8080-24 
  • BEARING, PTFE, 45/50 - 8067-105 
  • CONNECTOR, Beam, Connects 5/8 inch Motor Shaft to Chuck - 6472-156 
  • CHUCK, 28mm, Connects Beam Connector to Stirring Shaft - 6472-157 
  • COLLAR, with PTFE Gasket - 8127-28 
  • COIL, Cooling/Heating, Copper/PTFE, 1/2 inch - 12067-68 
  • ADAPTER, #15 - 29/42 (2) - 5030-42 
  • ADAPTER, #15 - 45/50 - 8042-21 
  • ADAPTER, #15 - 45/50, with 4 mm PTFE Stopcock - 5274-22 
  • ADAPTER, #11 and #15 - 45/50 - 5031-86 
  • ADAPTER, Side Arm, 45/50 - 45/50 - 24/40 - 5040-96 
  • ADAPTER, Angle, 45/50 - 45/50 - 5075-45 
  • ADAPTER, Offset, 45/50 - 45/50 - 5268-21 
  • BUSHING, Nylon, #11 - 7506-02 
  • BUSHING, Nylon, #15 (4) - 7506-06 
  • CONDENSER, 500 mm, 45/50 - 5945-76 
  • CONDENSER, Cold Finger, 14 mm O.D., 625 mm - 5958-99 
  • STOPPER, 45/50 (3) - 8250-20 
  • CLAMP, Chain - 11079-24 
  • CLAMP HOLDER, Pilot Plant (2) - 11081-21 
  • SUPPORT ROD,1/2 inch diameter, 18 inch long - 11166-25 
  • END-TO-END CONNECTOR - 11175-23 
  • GREASE, Krytox GPL - 8115-08 

Note: Product is shown with optional accessories.

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